专利号:US-5087759-A 优先权日:1989-02-08 标题:Synthesis of vicinal alkanedithiols 发明人:VALLEE YANNICK; LABAT YVES 权利人:ELF AQUITAINE 摘要:The invention relates to the manufacture of vicinal alkanedithiols from the corresponding alkylene trithiocarbonates. n The method according to the invention consists in treating alkylene trithiocarbonate with an alkaline sulfide, followed by acidification of the reaction medium. n The method is particularly well-suited for the synthesis of ethanedithiol from ethylene trithiocarbonate.
专利号:US-8115002-B2 优先权日:2006-09-20 标 题:Preparation of substituted morphinan-6-ones and salts and intermediates thereof 发明人:WANG PETER X; MOSER FRANK W; CANTRELL GARY L; GROTE CHRISTOPHER W 权利人:WANG PETER X; MOSER FRANK W; CANTRELL GARY L; GROTE CHRISTOPHER W; MALLINCKRODT LLC 摘要:The present invention is directed to processes for the synthesis of morphinan-6-ones and salts, intermediates, and analogs thereof.
专利号:US-8231848-B1 优先权日:2012-04-10 标题:One-pot synthesis of chalcopyrite-based semi-conductor nanoparticles 发明人:REN YUHANG; SUN CHIVIN; SHUM KAI 权利人:REN YUHANG; SUN CHIVIN; SHUM KAI; SUN HARMONICS LTD 摘要:Ternary and quaternary Chalcopyrite CuInxGa1-xSySe2-y (CIGS, where 0≰x and y≰1) nanoparticles were synthesized from molecular single source precursors (SSPs) by a one-pot reaction in a high boiling solvent using salt(s) (i.e. NaCl as by-product) as heat transfer agent via conventional convective heating method. The nanoparticles sizes were 1.8 nm to 5.2 nm as reaction temperatures were varied from 150° C. to 190° C. with very high-yield. Tunable nanoparticle size is achieved through manipulation of reaction temperature, reaction time, and precursor concentrations. In addition, the method developed in this study was scalable to achieve ultra-large quantities production of tetragonal and quaternary Chalcopyrite CIGS nanoparticles.
专利号:US-5565517-A 优先权日:1994-11-16 标题:Synthesis of organic polysulfide polymers 发明人:EFNER HOWARD F; SHAW JAMES E 权利人:PHILLIPS PETROLEUM CO 摘要:A process for preparing an organic polysulfide polymer, such as polyethylene trisulfide, is provided which comprises contacting a dimercaptan such as 1,2-ethanedithiol with elemental sulfur using a basic catalyst wherein the dimercaptan, elemental sulfur, and basic catalyst are each present in an effective amount to effect the preparation of the organic polysulfide polymer. A process for controlling the molecular weight of an organic polysulfide polymer is also provided which comprises contacting a mercaptan with a dimercaptan and sulfur, in the presence of a basic catalyst, under conditions sufficient to prepare an organic polysulfide polymer.
专利号:CN-114989235-A 优先权日:2015-09-28 标题:Design and synthesis of nucleotides based on novel disulfide linkers for use as reversible terminators for DNA sequencing by synthesis
专利号:CN-108779138-B 优先权日:2015-09-28 标题 :Design and synthesis of novel disulfide linker-based nucleotides for use as reversible terminators for DNA sequencing by synthesis
摘要:Schafer, E. W., Jr., and W. A. Bowles Jr. 1985. Acute oral toxicity and repellency of 933 chemicals to house and deer mice. Archives of Environmental Contamination and Toxicology 14:111-129. 摘要:Schafer, E. W., Jr., and W. A. Bowles Jr. 2004. Toxicity, Repellency of Phytotoxicity of 979 Chemicals to Birds, Mammals and Plants. Research Report No. 04-01. National Wildlife Research Center, Fort Collins, Colorado. 118 pp. https://www.aphis.usda.gov/ws/nwrc/chem-effects-db/U_schafer041_2004.pdf