CAS: 7721-01-9; Tantalum(V) Chloride

该化合物是一种无机化合物,其特点是深褐色至黑固态,是一种高度反应性和湿度高的物质,意味着它很容易吸收空气中的湿度;五氯丁二烯因其作为刘易斯酸的能力而闻名,它能够用于各种化学反应,特别是含有钽的化合物合成;它具有高熔点,在有机溶剂中溶解,但在水中是溶解的;该化合物通常由钽金属或钽氧化物的氯化产生;由于它具有再活性,必须谨慎处理五氯二苯,因为它与水和其他核分裂物发生激烈反应,释放盐酸和潜在的危险烟雾;它的应用包括用于生产基于钽的材料和作为有机合成的催化剂;由于它具有腐蚀性并具有潜在的健康危害,因此在与该化合物合作时,适当的安全防范措施是必不可少的.

结构式图片

欧盟法规

REACH注册ECHA物质ECHA物质C&L通报REACH预注册

上下游产品

CAS号7647-01-0 盐酸 | CAS号13569-72-7 tantalum tetrac... | CAS号15610-70-5 caesium tantalu... | CAS号67871-24-3 trichlorosulfon... | CAS号7783-71-3 氟化钽 | CAS号10294-34-5 三氯化硼 | CAS号7719-12-2 三氯化磷 | CAS号6074-84-6 乙醇钽(V) | CAS号18476-51-2 dichlorotantalu... | CAS号7721-01-9 五氯化钽 | CAS号7646-85-7 氯化锌 | CAS号10026-04-7 四氯化硅 | CAS号13597-22-3 tantalum oxytri... | CAS号850859-07-3 [(η3-1,3-(SiMe3... | CAS号1066-45-1 三甲基氯化锡 | CAS号850859-08-4 [(Me3SiCH=CHC(S... | CAS号7783-71-3 氟化钽

合成工艺路线路线简述

  • 合成目标产物 Tantalum(V) Chloride 主要起始原料 Hydrochloric Acid
  • (文献来源)合成步骤主要原料 Hydrochloric Acid
盐酸置于ta-Oxyd Hydrate体系中,用 Melt 作为反应溶剂,化学反应生成 五氯化钽
参考文献:Preparation Of The Refractory Metals By Fused Salt Electrolysis
标题:Preparation Of The Refractory Metals By Fused Salt Electrolysis

专利信息


专利号:US-7615169-B2
优先权日:2004-09-20
标题 :Method for synthesis of colloidal nanoparticles
发明人:STROUSE GEOFFREY FIELDING; GERBEC JEFFREY A; MAGANA DONNY
权利人:UNIV CALIFORNIA
摘要:A method for synthesis of high quality colloidal nanoparticles using comprises a high heating rate process. Irradiation of single mode, high power, microwave is a particularly well suited technique to realize high quality semiconductor nanoparticles. The use of microwave radiation effectively automates the synthesis, and more importantly, permits the use of a continuous flow microwave reactor for commercial preparation of the high quality colloidal nanoparticles.

专利号:US-7927516-B2
优先权日:2004-09-20
标题 :Method for synthesis of colloidal nanoparticles
发明人:STROUSE GEOFFREY F; GERBEC JEFFREY A; MAGANA DONNY
权利人:UNIV CALIFORNIA
摘要:A method for synthesis of high quality colloidal nanoparticles using comprises a high heating rate process. Irradiation of single mode, high power, microwave is a particularly well suited technique to realize high quality semiconductor nanoparticles. The use of microwave radiation effectively automates the synthesis, and more importantly, permits the use of a continuous flow microwave reactor for commercial preparation of the high quality colloidal nanoparticles.

专利号:US-2007074541-A1
优先权日:2003-10-10
标 题:Synthesis of germanium sulphide and related compounds
发明人:BADDING JOHN V; HEWAK DANIEL W; HUANG CHUNG-CHE
权利人:UNIV SOUTHAMPTON
摘要:The invention relates to synthesis of germanium sulphide glasses and optical devices formed therefrom. In a chemical vapour deposition process, germanium tetrachloride is reacted with hydrogen sulphide at temperatures in the range 450-700° C. to form germanium sulphide. Lower temperatures within this range of 450-550° C. directly produce a glass, whereas higher temperatures within the range of 600-700° C. produce a crystalline powder which can then be reduced to a glass by subsequent melting and annealing. The reaction is preferably carried out at atmospheric pressure or slightly higher. Thin films and bulk glasses suitable for optical waveguides can be formed directly in one processing step as can powders and microspheres. The materials synthesised are of a high purity with low oxide impurities and only trace levels of transition metal ions.

专利号:US-9919973-B1
优先权日:2017-03-31
标题 :Synthesis of high temperature ceramic powders
发明人:CHENG ZHE; FOROUGHI PANIZ; BEHRENS ANDRES
权利人:CHENG ZHE; FOROUGHI PANIZ; BEHRENS ANDRES; THE FLORIDA INTERNATIONAL UNIV BOARD OF TRUSTEES
摘要:The present invention relates to methods and apparatuses for forming high temperature ceramic powders. A method of producing high temperature ceramic powders according to an embodiment of the present invention can include preparing a solution, atomizing the solution, providing a gas and carrying the atomized solution into a furnace via the gas, evaporating the solvent, precipitating and drying the solutes, performing a thermolysis (or pyrolysis) reaction, and performing a carbothermal reduction reaction (CTR) in situ, and collecting product particles after they exit from the furnace.

专利号:US-4171320-A
优先权日:1977-10-19
标题 :Hydrocarbon synthesis from CO and H2 using Ru supported on group VB metal oxides
发明人:TAUSTER SAMUEL J; VANNICE M ALBERT
权利人:EXXON RESEARCH ENGINEERING CO
摘要:An improved method for the synthesis of hydrocarbons with reduced methane formation and for the selective generation of olefinic hydrocarbons, preferably C2-C5 olefins inclusive, which method comprises the steps of passing a CO and H2 synthesis gas stream over a catalyst at a temperature and pressure for a time sufficient to generate the desired olefinic products, wherein the improvement consists in using as a catalyst ruthenium on a support comprising at least one refractory Group VB metal oxide. The weight loading of the ruthenium may range from about 0.01 to about 15 wt. % based on the total catalyst weight. The ruthenium average crystallite size is preferably less than 5 nm (50A). The operating conditions of the instant process are typical for Fischer-Tropsch synthesis.

专利号:US-11713329-B2
优先权日:2018-12-10
标 题 :Intermediates useful in the preparation of halichondrin compounds and methods for preparing the same
发明人:XU WEIPING
权利人:BEIJING TIENYI LUFU PHARMATECH CO LTD
摘要:The invention relates to intermediates useful in the preparation of halichondrin compounds, methods for preparing the same and use thereof, such as halichondrins, eribulin, or their analogs. The intermediates, the methods and use thereof are used for the synthesis of the C20-C26 fragment of halichondrin compounds. The raw materials in the synthetic route of the invention are cheap and easily obtained, the sources and the qualities of the raw materials are reliable. The choice of the methods useful in the synthesis of chiral central structures are based on the structural characteristics of the reactants, thus effectively improving the synthesis efficiency, reducing the difficulties and risks of product quality control, and avoiding the use of highly toxic and expensive organotin catalysts to significantly decrease costs and improve environmental friendliness.
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合成参考文献


摘要:Masuda, T.; Shiotsuki, M.; Sanda, F., Science of Synthesis, (2010) 45, 1432.
摘要:Masuda, T.; Shiotsuki, M.; Sanda, F., Science of Synthesis, (2010) 45, 1436.
摘要:Roy, K.-M., Science of Synthesis, (2010) 47, 899.
摘要:Snaith, J. S., Science of Synthesis Knowledge Updates, (2011) 2, 181.
参考文献:10.1007/bf02257271
摘要:Pearce SR, Pich U, Harrison G, Flavell AJ, Heslop-Harrison JS, Schubert I, Kumar A. The Ty1-copia group retrotransposons of Allium cepa are distributed throughout the chromosomes but are enriched in the terminal heterochromatin. Chromosome Res. 1996 Aug;4(5):357–64. doi: 10.1007/bf02257271.
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