相似化合物
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pyridine n-Butyl chloride chlorosulfurous acid butyl ester diethyl ether N-butylpyridinium chloroaluminate 合成工艺路线路线简述
- 合成目标产物 1-Butylpyridinium Chloride 主要起始原料 Pyridine And 1-Chlorobutane
- (文献来源)合成步骤主要原料 Pyridine 和 1-Chlorobutane
吡啶,氯丁烷 反应 24.0H,以92%的收率获得n-正丁基氯化吡啶
参考文献:[hyetpy]Cl-h2O: An Efficient And Versatile Solvent System For The Dabco-Catalyzed Morita-baylis-hillman Reaction
标题:[hyetpy]Cl-h2O: An Efficient And Versatile Solvent System For The Dabco-Catalyzed Morita-baylis-hillman Reaction
摘要:一个非常高效和多功能的溶剂系统,[hyetpy]Cl-h2O,已经被开发并用于dabco催化的morita-baylis-hillman反应.
Doi:10.1039/c5Ra02102B
专利信息
专利号:US-2005087449-A1
优先权日:2002-03-04
标题:Electrochemical synthesis of ammonia
发明人:DENVIR ADRIAN; MURPHY OLIVER J; CISAR ALAN; ROBERTSON PRISCILLA; USELTON KYLE
摘要:A method for electrochemical synthesis of ammonia gas comprising providing an electrolyte between an anode and a cathode, providing hydrogen gas to the anode, oxidizing negatively charged nitrogen-containing species present in the electrolyte at the anode to form an adsorbed nitrogen species, and reacting the hydrogen with the adsorbed nitrogen species to form ammonia. Preferably, the hydrogen gas is provided to the anode by passing the hydrogen gas through a porous anode substrate. It is also preferred to produce the negatively charged nitrogen-containing species in the electrolyte by reducing nitrogen gas at the cathode. However, the negatively charged nitrogen-containing species may also be provided by supplying a nitrogen-containing salt, such as lithium nitride, into the molten salt electrolyte mixture in a sufficient amount to provide some or all of the nitrogen consumed in the production of ammonia.
专利号:US-2010191010-A1
优先权日:2007-07-02
标题 :Process for the synthesis of carbamates using co2
发明人:BOSMAN JORIS KAREL PETER; CARR ROBERT HENRY
权利人:HUNTSMAN INT LLC
摘要:Process for the synthesis of non cyclic carbamate derivatives from amine compounds, alcohols and CO 2 in the presence of ionic liquids and optionally in the presence of a base.
专利号:US-6712950-B2
优先权日:2002-03-04
标 题 :Electrochemical synthesis of ammonia
发明人:DENVIR ADRIAN; MURPHY OLIVER J; CISAR ALAN; ROBERTSON PRISCILLA; USELTON KYLE
权利人:LYNNTECH INC
摘要:A method for electrochemical synthesis of ammonia gas comprising providing an electrolyte between an anode and a cathode, providing hydrogen gas to the anode, oxidizing negatively charged nitrogen-containing species present in the electrolyte at the anode to form an adsorbed nitrogen species, and reacting the hydrogen with the adsorbed nitrogen species to form ammonia. Preferably, the hydrogen gas is provided to the anode by passing the hydrogen gas through a porous anode substrate. It is also preferred to produce the negatively charged nitrogen-containing species in the electrolyte by reducing nitrogen gas at the cathode. However, the negatively charged nitrogen-containing species may also be provided by supplying a nitrogen-containing salt, such as lithium nitride, into the molten salt electrolyte mixture in a sufficient amount to provide some or all of the nitrogen consumed in the production of ammonia.
专利号:US-6881308-B2
优先权日:2002-03-04
标 题 :Electrochemical synthesis of ammonia
发明人:DENVIR ADRIAN J; MURPHY OLIVER J; CISAR ALAN J; ROBERTSON PRISCILLA; USELTON KYLE
权利人:LYNNTECH INC
摘要:A method for electrochemical synthesis of ammonia gas comprising providing an electrolyte between an anode and a cathode, providing hydrogen gas to the anode, oxidizing negatively charged nitrogen-containing species present in the electrolyte at the anode to form an adsorbed nitrogen species, and reacting the hydrogen with the adsorbed nitrogen species to form ammonia. Preferably, the hydrogen gas is provided to the anode by passing the hydrogen gas through a porous anode substrate. It is also preferred to produce the negatively charged nitrogen-containing species in the electrolyte by reducing nitrogen gas at the cathode. However, the negatively charged nitrogen-containing species may also be provided by supplying a nitrogen-containing salt, such as lithium nitride, into the molten salt electrolyte mixture in a sufficient amount to provide some or all of the nitrogen consumed in the production of ammonia.
专利号:US-8608935-B2
优先权日:2006-03-24
标 题:Apparatus and method for synthesis of alane
发明人:VAJO JOHN J; LIU PING
权利人:VAJO JOHN J; LIU PING; GM GLOBAL TECH OPERATIONS INC
摘要:One embodiment of the invention includes an electrochemical cell and an externally applied electrical potential used to drive a direct synthesis reaction to produce alane.
专利号:US-9512080-B2
优先权日:2012-07-10
标 题:Synthesis of acridinium compounds by N-alkylation of acridans
发明人:NATRAJAN ANAND; WEN DAVID
权利人:SIEMENS HEALTHCARE DIAGNOSTICS INC
摘要:A method is provided for N-alkylation of acridine compounds by reduction of acridines to corresponding acridans to improve the reactivity of the acridine nitrogen, and subsequent N-alkylation of the acridans in ionic liquid solvents to provide the corresponding acridinium compounds in high yield. This inventive process improves chemical conversion, and does not require the use of highly toxic alkylating agents, such as 1,3-propane sultone.