1-十四烯置于potassium Permanganate,硫酸,溶剂黄146体系中,用 二氯甲烷,水 作为反应溶剂,化学反应 21.0H,以83%的收率获得产物十三酸 参考文献:Carboxylic Acids From The Oxidation Of Terminal Alkenes By Permanganate: Nonadecanoic Acid 标题:Carboxylic Acids From The Oxidation Of Terminal Alkenes By Permanganate: Nonadecanoic Acid 摘要: DOI:10.15227/orgsyn.060.0011
专利号:US-3872168-A 优先权日:1972-10-02 标题:Synthesis of acids and amides 发明人:COLLMAN JAMES P; WINTER STANLEY R; KOMOTO ROBERT G 权利人:TRUSTEES OF THE LELAND STAMFOR 摘要:Synthesis of acids R1COOH and amides R1CONR2R3 wherein R1 is attached to the carbonyl group by an aliphatic carbon atom and R2 and R3 are hydrogen or organic groups of a primary or secondary amine, by forming an alkyl or acyl intermediate (R1Fe(CO) 4 or R1COFe(CO) 4) and treating the intermediate with a suitable cleaving agent and, in the case of amides, also with ammonia or an amine.
专利号:US-9643915-B2 优先权日:2013-03-15 标题:Methods for the synthesis of sphingomyelins and dihydrosphingomyelins 发明人:ONICIU DANIELA CARMEN; HECKHOFF STEFAN; OSWALD BENOIT; REBMANN PETER; PEER ANDREAS; GONZALEZ MIGUEL; SAUTER PATRIK 权利人:CERENIS THERAPEUTICS HOLDING SA 摘要:The present invention includes methods for the synthesis of sphingomyelins and dihydrosphingomyelins. The present invention also includes methods for the synthesis of sphingosines and dihydrosphingosines. The present invention further includes methods for the synthesis of ceramides and dihydroceramides.
专利号:US-9708354-B2 优先权日:2013-03-15 标 题:Methods for the synthesis of sphingomyelins and dihydrosphingomyelins 发明人:ONICIU DANIELA CARMEN; HECKHOFF STEFAN; OSWALD BENOIT; REBMANN PETER; PEER ANDREAS; GONZALEZ MIGUEL; SAUTER PATRIK 权利人:CERENIS THERAPEUTICS HOLDING SA 摘要:The present invention includes methods for the synthesis of sphingomyelins and dihydrosphingomyelins. The present invention also includes methods for the synthesis of sphingosines and dihydrosphingosines. The present invention further includes methods for the synthesis of ceramides and dihydroceramides.
专利号:US-5723619-A 优先权日:1997-01-13 标 题 :Method for the synthesis of deoxypyridinoline 发明人:HATCH ROBERT P 权利人:BAYER AG 摘要:Disclosed is a method for the chemical synthesis of deoxypyridinoline (DPD). The synthesis involves the preparation of a protected 3-hydroxypyridinium starting with a Nα-protected lysine and a 5,6-epoxy-2-N-protected-O-protected-(2S)-2-aminohexanoate with subsequent deprotection to provide the desired DPD.
专利号:US-9957355-B2 优先权日:2013-06-12 标 题 :Device and method for synthesis of a polymer under separation of a gaseous substance 发明人:ZHU NING; STAMMER ACHIM; CLAUSS JOACHIM; KORY GAD 权利人:BASF SE 摘要:The invention relates to a device for synthesis of a polymer under separation of a gaseous substance. Said device comprises a reaction chamber ( 1 ), which has a top section ( 11 ), a middle section ( 12 ) and a bottom section ( 13 ), an inlet opening ( 2 ) which is arranged in the middle section ( 12 ), a first outlet opening ( 3 ) which is arranged in the bottom section ( 13 ), a second outlet opening ( 4 ) which is arranged in the top section ( 11 ), a first return opening ( 51 ), which is arranged in the bottom section ( 13 ), a second outlet opening ( 52 ), which is arranged under the top section ( 11 ), a distribution device ( 6 ), which is arranged between the top section ( 11 ) and the middle section ( 12 ), and a removal device ( 7 ) which is arranged to be movable along the top section ( 11 ). The invention further relates to a method for synthesis of a polymer which can be carried out in said device.
专利号:US-7767425-B2 优先权日:2001-11-16 标 题:Enzymatic synthesis of sugar acrylates 发明人:BOECKH DIETER; HAUER BERNHARD; HAERING DIETMAR 权利人:BASF AG 摘要:A process is described for the enzymatic synthesis of sugar acrylates, and a process is described for preparing polymeric sugar acrylates, the polymers obtainable by this process and their use for preparing, for example, cosmetics, drugs, laundry detergents, thickeners, protecting colloids, superabsorbents and textile sizes.
[参考文献]: Jin X, Et, Al. Undecanoic Acid, Lauric Acid, And N-Tridecanoic Acid Inhibit Escherichia Coli Persistence And Biofilm Formation. J Microbiol Biotechnol. 2020 Oct 13. [参考文献]: Bashar Amer, Et Al. Direct Derivatization Vs Aqueous Extraction Methods Of Fecal Free Fatty Acids For Gc-Ms Analysis. Lipids. 2015 Jul;50(7):681-9. [参考文献]: Jacqueline C Lieblein-Boff, Et Al. Exploratory Metabolomic Analyses Reveal Compounds Correlated With Lutein Concentration In Frontal Cortex, Hippocampus, And Occipital Cortex Of Human Infant Brain. Plos One. 2015 Aug 28;10(8):E0136904. [参考文献]: Janclei P Coutinho, Et Al. Use Of Multivariate Statistical Techniques To Optimize The Separation Of 17 Capsinoids By Ultra Performance Liquid Chromatography Using Different Columns. Talanta. 2015 Mar:134:256-263. [参考文献]: Jonathan Y Bernard, Et Al. The Association Between Linoleic Acid Levels In Colostrum And Child Cognition At 2 And 3 Y In The Eden Cohort. Pediatr Res. 2015 Jun;77(6):829-35.
合成参考文献
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