CAS: 24413-04-5; P-(Trimethoxysilyl)Benzyl Chloride

三氯[4-(氯甲基)苯基]硅烷,甲醇,N,N-二异丙基乙胺 以91%的收率获得
参考文献:Carpino,L. A.;Mansour,E. M. E.;Knapczyk,J.,J. Org. Chem.,1983,48,N 5,666-669
标题:Carpino,L. A.;Mansour,E. M. E.;Knapczyk,J.,J. Org. Chem.,1983,48,N 5,666-669

专利信息

专利号:US-2010098623-A1
优先权日:2007-02-07
标 题 :Zeolite materials and synthesis method thereof
发明人：GAGEA BOGDAN; JACOBS PIERRE; MARTENS JOHAN; VANDEPITTE HANS
权利人:GAGEA BOGDAN; JACOBS PIERRE; MARTENS JOHAN; VANDEPITTE HANS
摘要:The present invention provides zeolites and zeolite-like material having an enhanced microporosity. It was found that such zeolites can be obtained using a zeolite synthesis method comprising the preparation of a gel or solution for the synthesis of a zeolite, said gel or solution comprising appropriate amounts of (i) a conventional monomeric or polymeric silica source and (ii) a molecular template as a microstructuring agent, characterized in that said gel or solution further comprises an organosilane compound having limited self-assembling capacity.

专利号:US-2005261474-A1
优先权日:2004-05-20
标题:Method of support-based chemical synthesis
发明人：HOUGHTEN RICHARD A; YU YONGPING
权利人:MIXTURE SCIENCES INC
摘要:A method of synthesis on a solid phase support is disclosed that provides a cleaved product containing a protecting group that would have been cleaved by reaction with anhydrous HF wherein the support is volatilized during cleavage of the protected product from the support by reaction with diluted HF.

专利号:WO-03068806-A1
优先权日:2002-02-14
标 题 :Solid phase peptide synthesis on silica
发明人：GROARKE MICHELLE
权利人:JOHNSON MATTHEY PLC; GROARKE MICHELLE
摘要:A method for peptide synthesis is described, comprising steps of forming an organofunctional silica by reaction of an alkyl silicate, an organofunctional silane and water, optionally in the presence of a template compound; removing the template compound if present; reacting said organofunctional silica with a first protected amino acid to produce a tethered protected amino acid; deprotecting the tethered protected amino acid; reacting at least one further protected amino acid with said tethered deprotected amino acid to form a tethered peptide, and removing the peptide from the organofunctional silica. Preferably, prior to reaction of the first protected amino acid, the organofunctional silica is reacted with at least one linking compound to form a linker-modified organofunctional silica with which the first protected amino acid is reacted. A method for preparing an organfunctional silica by the co-hydrolysis of an alkyl silicate and an organofunctional silane is depicted below. The wavy line represents the silicon atom on or within the resulting silica material formula (I). A reaction of a protected amino acid with an organofunctional silica to provide a tethered protected amino acid is depicted below formula (II).

专利号:US-9895673-B2
优先权日:2015-12-01
标题:Functionalized surfaces and preparation thereof
发明人：PECK BILL JAMES; INDERMUHLE PIERRE; MARSH EUGENE P; FERNANDEZ ANDRES; STERN DAVID
权利人:TWIST BIOSCIENCE CORP
摘要:Compositions, devices, methods and systems are provided for differential functionalization of a surface of a structure to support biopolymer synthesis. Provided herein are processes which include use of lamps, lasers, and/or microcontact printing to add functional groups to surfaces for the efficient and uniform synthesis of oligonucleic acids.

专利号:US-7205161-B2
优先权日:2001-01-10
标 题 :Polymer brushes for immobilizing molecules to a surface or substrate having improved stability
发明人：KLAERNER GERRIT; BENOIT DIDIER; CHARMOT DOMINIQUE; NOMULA SRINIVAS; PIOTTI MARCELO EDUARDO; MAZZOLA LAURA T
权利人:SYMYX TECHNOLOGIES INC
摘要:Sensors for determining the presence and concentration of biomolecules in a biological sample are provided in the form of polymer brushes, which comprise a substrate having a surface modified with a hydrophobic polymer segment, attached to which is a water-dispersible or water-soluble polymer segment having functional groups that bind probes. The method of synthesis of such sensors preferably includes use of controlled free radical polymerization techniques, which allows for controlled architecture polymers to modify the surface of the substrate, and the use of monomers possessing functional groups which do not require activation prior to probe attachment. In this manner functional groups in the polymer chain are removed from the surface, which allows for solution chemistry to be more realistically reproduced with the benefits of a solid bound probe.

专利号:US-9834536-B2
优先权日:2013-04-23
标题:Method for producing catalyst for cyclic carbonate synthesis
发明人：TAKAHASHI TOSHIKAZU; YASUDA HIROYUKI; SAKAKURA TOSHIYASU; YAMAMOTO SHOUJI; NANIKI TAKASHI; FURUKAWA TAKURO
权利人:AIST; MARUZEN PETROCHEM CO LTD
摘要:A method for producing a heterogeneous catalyst for use of synthesizing cyclic carbonates by reacting an epoxide and carbon dioxide in the presence of the catalyst. A method for making a catalyst that includes forming a catalyst precursor then reacting the catalyst precursor with a tertiary phosphine.