磷酸三乙酯,1,2-二溴乙烷 反应 5.0H,反应生成 2-溴乙基膦酸二乙酯 参考文献:Synthesis And Characterization Of Aminophosphonates Zirconium As New Mesoporous Materials 标题:Synthesis And Characterization Of Aminophosphonates Zirconium As New Mesoporous Materials 摘要:一系列具有不同碳链长度的氨基膦酸锆化合物(n=2-6)首次合成.这些化合物通过ft-Ir,Sem,Tem,Tg和氮吸附-脱附进行表征.根据实验数据,这些材料不仅具有类似于磷酸锆的层状结构介孔和非常好的热稳定性,而且可以调节层间距离,孔径和孔体积.因此,氨基膦酸锆具有特殊的优异性能,并将具有潜在的应用前景. DOI:10.1155/2012/640317
专利号:US-2008312430-A1 优先权日:2004-10-20 标题:Method of Preparing or Synthesizing Polyazamacrocycle Derivatives 发明人:CIHELNIK SIMON; DROZ LADISLAV; SRAMEK MARTIN 权利人:THERAPHARM GMBH 摘要:The present invention relates to novel processes for the synthesis of polyazamacrocycle derivatives. Furthermore, the present invention relates to novel polyazamacrocycle derivatives as well as novel intermediates for the synthesis of said polyazamacrocycle derivatives.
专利号:US-6531470-B1 优先权日:1998-01-23 标题:Oxazolidinone combinatorial libraries, compositions and methods of preparation 发明人:GORDEEV MIKHAIL F; LUEHR GARY W; PATEL DINESH V; NI ZHI-JIE; GORDON ERIC 权利人:UPJOHN CO 摘要:Oxazolidinones and methods for their synthesis are provided. Also provided are combinatorial libraries comprising oxazolidinones, and methods to prepare the libraries. Further provided are methods of making biologically active oxazolidinones as well as pharmaceutically acceptable compositions comprising the oxazolidinones. The methods of library preparation include the attachment of oxazolidinones to a solid support. The methods of compound preparation in one embodiment involve the reaction of an iminophosphorane with a carbonyl containing polymeric support.
专利号:US-6562844-B2 优先权日:1998-01-23 标 题:Oxazolidinone combinatorial libraries, compositions and methods of preparation 发明人:GORDEEV MIKHAIL F; LUEHR GARY W; PATEL DINESH V; NI ZHI-JIE; GORDON ERIC 权利人:UPJOHN CO 摘要:Oxazolidinones and methods for their synthesis are provided. Also provided are combinatorial libraries comprising oxazolidinones, and methods to prepare the libraries. Further provided are methods of making biologically active oxazolidinones as well as pharmaceutically acceptable compositions comprising the oxazolidinones. The methods of library preparation include the attachment of oxazolidinones to a solid support. The methods of compound preparation in one embodiment involve the reaction of an iminophosphorane with a carbonyl containing polymeric support.
专利号:US-7002020-B1 优先权日:1998-01-23 标题:Oxazolidinone combinatorial libraries, compositions and methods of preparation 发明人:GORDEEV MIKHAIL F; LUEHR GARY W; PATEL DINESH V 权利人:UPJOHN CO 摘要:Oxazolidinones and methods for their synthesis are provided. Also provided are combinatorial libraries comprising oxazolidinones, and methods to prepare the libraries. Further provided are methods of making biologically active oxazolidinones as well as pharmaceutically acceptable compositions comprising the oxazolidinones. The methods of library preparation include the attachment of oxazolidinones to a solid support. The methods of compound preparation in one embodiment involve the reaction of an iminophosphorane with a carbonyl containing polymeric support.
专利号:CN-103374035-A 优先权日:2012-04-24 标 题:A method for microwave synthesis of organic phosphine functionalized imidazole ionic liquids
专利号:CN-103374035-B 优先权日:2012-04-24 标 题 :A method for microwave synthesis of organic phosphine functionalized imidazole ionic liquids