Alkaline Earth Salt Of/the/ Methylsulfuric Acid 200.0 °C,2.67 Kpa 条件下,反应生成氘代二甲亚砜 参考文献:Cotton Et Al.,Journal Of The Chemical Society,1959,P. 4138 标题:Cotton Et Al.,Journal Of The Chemical Society,1959,P. 4138
专利号:US-2022411943-A1 优先权日:2021-06-23 标 题 :Process for the Electrochemical Synthesis of Green Urea, an Electrochemical Cell for the Electrochemical Synthesis of Green Urea and the Green Urea Produced Thereby 发明人:GHORAI UTTAM KUMAR; MUKHERJEE Jit; PAUL SOURAV; ADALDER ASHADUL 权利人:GHORAI UTTAM KUMAR; RAMAKRISHNA MISSION VIDYAMANDIRA 摘要:This invention relates to a process for the electrochemical synthesis of green urea, and the urea produced thereby. The electrochemical synthesis of urea involves the reduction of dual purging gases N 2 and CO 2 via six electron transfer process (N 2 +CO 2 +6H + +6e − →CO (NH 2 ) 2 +H 2 O) & reduction of the NO 3 − ions and CO 2 via sixteen electron transfer process (2NO 3 −+CO 2 +18H + +16e − →CO(NH 2 ) 2 +7H 2 O) under ambient condition using copper phthalocyanine (CuPc) catalyst. The binding of two intermediate products during dual reduction simultaneously, leads to the production of urea in water medium under ambient conditions.
专利号:US-11891375-B2 优先权日:2021-07-26 标 题 :Method for the synthesis of 2,4-dimethylpyrimidin-5-ol, intermediates, and method for the synthesis of Lemborexant using the intermediates 发明人:AKHATOU ABDESLAM; DOBARRO RODRÃ?GUEZ ALICIA 权利人:MOEHS IBERICA SL 摘要:A method is for the synthesis of 2,4-dimethylpyrimidin-5-ol, which can be used as an intermediate compound in the synthesis of Lemborexant. The method includes reacting a nitrophenyl compound with N,N-dimethylformamide diethyl acetal.
专利号:US-7294486-B2 优先权日:2001-09-05 标 题:Enzymatic process for the synthesis of organo-fluorine compounds 发明人:O'HAGAN DAVID; SCHAFFRATH CHRISTOPH 权利人:UNIV ST ANDREWS 摘要:There is described a process for the synthesis of a fluoronucleoside compound, said process comprising mixing a substrate and an enzyme from Streptomyces cattelya as catalyst. The process may be used to produce an 18 F labelled fluoronucleoside compound. There is also described an enzyme derived from Streptomyces cattelya which has the capacity to catalyse the synthesis of a fluoronucleoside compound.
专利号:US-9476071-B2 优先权日:2013-02-28 标 题 :Process for the enzymatic synthesis of (7S)-3,4-dimethoxybicyclo[4.2.0]OCTA-1,3,5-triene-7-carboxylic acid and application in the synthesis of ivabradine and salts thereof 发明人:PEDRAGOSA-MOREAU SANDRINE; LEFOULON FRANÇOIS 权利人:SERVIER LAB 摘要:Process for the enzymatic synthesis of the compound of formula (I): n ncomprising enantioselective enzymatic hydrolysis of the nitrile of formula (IV):n n nusing the nitrilase of Rhodococcus rhodochrous of EMBL accession number EF467367.1, and the application of such a process in the synthesis of ivabradine and addition salts thereof with a pharmaceutically acceptable acid.
专利号:WO-2023102600-A1 优先权日:2021-12-06 标题:Synthesis of amphiphilic block copolymers and polymeric nanofibers produced therefrom 发明人:ZETTERLUND PER B; ISHIZUKA FUMI; KIM HYUN JIN; CHATANI SHUNSUKE; NIINO HIROSHI 权利人:NEWSOUTH INNOVATIONS PTY LTD 摘要:The present disclosure relates to the field of synthesis of block copolymers, and polymeric nanofibers having a core-shell morphology produced therefrom. The present disclosure relates to the field of synthesis of block copolymers where one block is more hydrophobic than the other block and is a different composition. The disclosure also relates to uses of these polymeric nanofibers in various applications, such as reinforcing a polymeric matrix and for coatings applications.
专利号:EP-0842924-B1 优先权日:1996-11-14 标 题 :Pyridine intermediates, useful in the synthesis of beta-adrenergic receptor agonists 发明人:WRIGHT STEPHEN WAYNE 权利人:PFIZER 摘要:The present invention relates to certain compounds of the formula (I), which are useful in the synthesis of certain beta -adrenergic receptor agonists. The invention also relates to a process for synthesizing the compounds of formula (I) and to compounds of the formula (II), wherein R<1>, R<2> and R<4> are defined herein, which are useful in the synthesis of the compounds of formula (I). The invention also relates to a process for synthesizing a compound of formula (II). The invention further relates to processes for synthesizing compounds of formula (Z*), R<1>, R<2> and Y<2*> are defined herein.o
参考标题:Cobalt-Catalyzed Allylation Of Amides With Styrenes Using Dmso As Both The Solvent And The α-Methylene Source 作者:Xu Zhang,Zhi Zhou,Huiying Xu,Xuefeng Xu,Xiyong Yu,Wei Yi |发布日期:2019.9.20 摘要:An Efficient Synthesis Of Privileged Allylic Amines Has Been Developed Via Cobalt-Catalyzed Allylation Of Amides With Styrenes, In Which Dmso Was Used As Both The Solvent And The α-Methylene Source. This Transformation Features High Yields, And Selectivity For The (E)-Isomer Of The Linear Product. Through The Experimental And Computational Investigations, A Sequential K2S2O8-Mediated Oxidative Cou
合成参考文献
参考文献:10.1007/s00253-011-3444-7 摘要:Li XF, Zhu Z, Zhao GL, Yu YG, Lai FR, Wu H. A novel biocatalytic approach to acetylation of 1-β-D-arabinofuranosylcytosine by Aspergillus oryzae whole cell in organic solvents. Appl Microbiol Biotechnol. 2012 Jan;93(1):143–50. doi: 10.1007/s00253-011-3444-7.