594-31-0 + 148-18-5 = 603-36-1 + 97-77-8 反应条件:1.1 Solvents: Toluene; 3 H,100 °C 标题:Synthesis And Structure Of Tetraphenylantimony N,N-Diethyldithiocarbamate 作者:Sharutin,V. V.; Et Al 参考文献:Russian Journal Of General Chemistry (Translation Of Zhurnal Obshchei Khimii) 日期:2002 卷标:72(9) 页码:1379-1382
三氟化锑置于phli Or Phmgbr体系中,用 Not Given 作为反应溶剂,化学反应生成 三苯基锑 参考文献:Bone,Stephen P.; Sowerby,D. Bryan,Journal Of The Chemical Society,Dalton Transactions 标题:Bone,Stephen P.; Sowerby,D. Bryan,Journal Of The Chemical Society,Dalton Transactions
专利号:US-2018076373-A1 优先权日:2016-09-13 标题 :SOLUTION PHASE SYNTHESIS OF HIGHLY PROCESSIBLE NANOCRYSTALLINE LiZnP AND SIMILAR TERNARY SEMICONDUCTORS 发明人:Vela-Becerra Javier; White Miles Arthur Burris; THOMPSON MICHELLE JOANN; MILLER GORDON J 权利人:VELA BECERRA JAVIER; White Miles Arthur Burris; THOMPSON MICHELLE JOANN; MILLER GORDON J; UNIV IOWA STATE RES FOUND INC 摘要:Nowotny-Juza phases offer a wide range of potential applications including solar cell and thermoelectric device fabrication. The disclosure presents a solution phase synthesis of the Nowotny-Juza semiconductors LiZnP, LiCdP, and LiZnSb. These samples are phase pure, crystalline, and exhibit particle sizes of around 20 nm.
专利号:US-4374291-A 优先权日:1981-11-06 标题:Synthesis of bis(ethynylphenyl) compounds 发明人:LAU KREISLER S Y 权利人:HUGHES AIRCRAFT CO 摘要:Bis(ethynylphenyl) compounds are prepared by an improved synthesis process which increases yield and is suitable for large scale synthesis operations. Aromatic dianilines are diazotized to form aromatic halides that are subsequently coupled with an end-protecting group having acetylenic moieties. The end-protecting groups are subsequently removed leaving the desired diethynyl derivative in quantitative yields.
专利号:US-3673250-A 优先权日:1970-12-01 标 题 :Catalytic hydration of nitriles to produce amides 发明人:RAUCH FRANCIS CLYDE; NACHTIGALL GUENTER WILLI 权利人:AMERICAN CYANAMID CO 摘要:Catalytic hydration of a nitrile with water in presence of a homogeneous catalyst in solution with the reactants, is described for the synthesis of an amide. The catalyst comprises two components, one a transition metal compound such as a rhodium compound, the other an organic phosphite, phosphine, arsenite, arsine, stibine or antimonite. One preferred example is rhodium trichloride with triphenyl phosphine as a catalyst for hydration of acrylonitrile to acrylamide. Some complexing of the solution components is suggested. In some embodiments, presence of a further component such as triphenyl phosphine oxide will improve the process.
专利号:US-3641082-A 优先权日:1969-02-17 标题 :Process for the alkylation alkenylation or arylation of heavy-metla salts by means of organo-triptychsiloxazolidines 发明人:MULLER RICHARD; FREY HANS; DATHE CHRISTIAN 权利人:INST SILIKON & FLUORKARBONCHEM 摘要:PROCESS FOR THE ALKYLATOR, XXXVLATION OR ARYLATION OF SALTS OR HYDROXIDES OF HEAVY METALS, SUCH AS MERCURY, BXXOUTH, ANTIMONY AND XXX COMPRISING REACTING THEM WITH ORGANO-TRIPTYCH-SILEXXOLIDINES IN THE PRESENCE OF FLUORINE. THE PRODUCTS ACCORDING TO THIS INVENTION ARE USEFUL AS PHARMACEUTICALS AND PESTICIDES, AND MAY ALSO SERVE IN THE SYNTHESIS OF OTHER USEFUL PRODUCTS.
专利号:US-5342909-A 优先权日:1992-04-03 标题:Ruthenium and osmium metal carbene complexes for olefin metathesis polymerization 发明人:GRUBBS ROBERT H; JOHNSON LYNDA K; NGUYEN SONBINH T 权利人:CALIFORNIA INST OF TECHN 摘要:Processes for the synthesis of several new carbene compounds of ruthenium and osmium are provided. These novel complexes function as stable, well-defined catalysts for the metathesis polymerization of cyclic olefins.
专利号:US-10333045-B2 优先权日:2015-09-01 标题 :Solution based synthesis of copper-arsenic-chalcogen derived nanoparticles 发明人:AGRAWAL RAKESH; BOUDOURIS BRYAN WILLIAM; BALOW ROBERT B 权利人:AGRAWAL RAKESH; BOUDOURIS BRYAN WILLIAM; BALOW ROBERT B; PURDUE RESEARCH FOUNDATION 摘要:A method for obtaining copper arsenic chalcogen derived nanoparticles, including selecting a first precursor material from the group comprising copper, arsenic, antimony, bismuth, and mixtures thereof, selecting a second material from the group comprising sulfur, selenium, tellurium, and mixtures thereof, and then reacting both precursors in a solvent medium at conditions conducive to the formation of copper arsenic chalcogen derived nanoparticles.
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