CAS: 84-47-9; 2-(Tert-Butyl)Anthracene-9,10-Dione
该化合物是炭疽的衍生物,其特点是在2位置上存在一个三丁基乙酮组,这种改变增强了其稳定性和溶性,使其作为有机合成和工业应用的中间体特别有用,其主要优点包括高纯度,红氧化反应的连续性能和适合通过炭疽过程用于过氧化氢生产.三丁基磷还改进了催化工艺中的选择性,减少了不必要的副产品.由于其强大的化学结构,它表现出极好的热和氧化稳定性,确保了在高要求环境中的可靠性能.该化合物被广泛用于精细的化学和制药生产.
物理性质
MSDS等安全信息
欧盟法规
ECHA物质C&L通报REACH预注册上下游产品
2-Benzoyl-4-tert-butylbenzoic acid 2-( 4'-tert-butylbenzoyl)benzoic acid 5-t-Butyl-2-benzoylbenzoesaeure tert-butyl-anthrone2-tert-butyl-anthrone 2-(t-butyl)anthracene 2,6-di-tert-butylanthracene-9,10(4aH,9aH)-dione 9,10-bis(4-bromophenyl)-2-tert-butyl-9,10-dihydroxy-9,10-dihydroanthracene 2-tert-butyl-9,10-bis(4-bromophenyl)anthracene合成工艺路线路线简述
- 18801-00-8 = 84-47-9
反应条件:1.1 Reagents: Potassium Peroxymonosulfate Sulfate (2Khso5.Khso4.K2So4) Catalysts: Iodobenzene,Ferrate(4-),Chloro[[4,4′,4′′,4′′′-(21H,23H-Porphine-5,10,15,20-Tetrayl-Kn21,Kn2... Solvents: Acetonitrile,Water; 3 H,Rt
标题:Metalloporphyrin/iodine(Iii)-Cocatalyzed Oxygenation Of Aromatic Hydrocarbons
作者:Yoshimura,Akira; Et Al
参考文献:Advanced Synthesis & Catalysis 日期:2010 卷标:352(9) 页码:1455-1460]
31592-26-4 = 84-47-9
反应条件:1.1 Reagents: Sulfuric Acid
标题:Synthesis Of Tert-Butylanthraquinones
作者:Pozdnyakovich,Yu. V.; Et Al
参考文献:Zhurnal Organicheskoi Khimii 日期:1986 卷标:22(3) 页码:595-601]
917-92-0 + 54160-73-5 = 84-47-9
反应条件:1.1 Catalysts: Chloro[(1,2,5,6-η)-1,5-Cyclooctadiene][(1,2,3,4,5-η)-1,2,3,4,5-Pentamethyl-2,4-C... Solvents: 1,2-Dichloroethane; 6 H,Rt
标题:Ru(Ii)-Catalyzed [2+2+2] Cycloaddition Of 1,2-Bis(Propiolyl)Benzenes With Monoalkynes Leading To Substituted Anthraquinones
作者:Yamamoto,Yoshihiko; Et Al
参考文献:Chemical Communications (Cambridge 日期:2003 卷标:(11) 页码:1290-1291]
18801-00-8 = 84-47-9 + 1240519-79-2 + 1240519-80-5
反应条件:1.1 Reagents: Iodine(2+),Bis[(Hydroxy-Ko)Phenyliodoniumato]Phenyl-,Sulfate (1:2) Catalysts: Bis(Methanol)-μ-Oxobis[c,C,C-Tris(1,1-Dimethylethyl)-29H,31H-Tribenzo[b,G,L]Pyri... Solvents: Methanol; 0.5 H,25 °C
标题:Binuclear Iron(Iii) Phthalocyanine(μ-Oxo-Dimer)-Catalyzed Oxygenation Of Aromatic Hydrocarbons With Iodosylbenzene Sulfate And Iodosylbenzene As The Oxidants
作者:Neu,Heather M.; Et Al
参考文献:Advanced Synthesis & Catalysis 日期:2009 卷标:351(18) 页码:3168-3174]
18801-00-8 = 84-47-9
反应条件:1.1 Reagents: Iodosylbenzene Catalysts: Ferrate(2-),μ-Oxobis[2,9,16,23-Tetrakis(1,1-Dimethylethyl)-29H,31H-Phthalocyani... Solvents: Dichloromethane; 24 H,Rt
标题:Transition Metal-Mediated Oxidations Utilizing Monomeric Iodosyl- And Iodylarene Species
作者:Yusubov,Mekhman S.; Et Al
参考文献:Tetrahedron 日期:2010 卷标:66(31) 页码:5745-5752]
98-06-6 = 84-47-9
反应条件:1.1 Reagents: Aluminum Chloride,Sulfuric Acid Solvents: Water; 32 Min,95 - 110 °C
标题:Facile,Efficient And One-Pot Synthesis Of Anthraquinone Derivatives Catalyzed By Alcl3/h2So4 Under Heterogeneous And Mild Conditions
作者:Hossei,Naeimi; Et Al
参考文献:Cuihua Xuebao 日期:2008 卷标:29(1) 页码:86-90]
98-06-6 = 84-47-9
反应条件:1.1 Catalysts: Methanesulfonic Acid,Aluminum Chloride; 37 Min,95 - 100 °C
标题:Rapid,Efficient And One Pot Synthesis Of Anthraquinone Derivatives Catalyzed By Lewis Acid/methanesulfonic Acid Under Heterogeneous Conditions
作者:Naeimi,Hossein; Et Al
参考文献:Dyes And Pigments 日期:2009 卷标:81(3) 页码:259-263]
146-81-6 = 84-47-9
反应条件:1.1 40 Min,573 K; 573 K -> Rt
标题:Green Synthesis Of 2-Tert-Butylanthraquinone By Dehydration Of 2-(4-Tert-Butylbenzoyl)Benzoic Acid Over Y Zeolites
作者:Liu,Min; Et Al
参考文献:Preprints - American Chemical Society 日期:2008 卷标:53(1) 页码:225-226]
62262-26-4 = 84-47-9
反应条件:1.1 Reagents: Nitric Acid Solvents: Water; 6.5 H,Reflux2.1 Reagents: Sulfuric Acid
标题:Synthesis Of Tert-Butylanthraquinones
作者:Pozdnyakovich,Yu. V.; Et Al
参考文献:Zhurnal Organicheskoi Khimii 日期:1986 卷标:22(3) 页码:595-601]
146-81-6 = 84-47-9 + 412300-88-0
反应条件:1.1 Reagents: 1-Carboxy-4-Hydroxy-α-Oxo-2,5-Cyclohexadiene-1-Propanoic Acid Solvents: Benzene
标题:The Polymerization Of O-(P-Toluyl)Benzoic Acid
作者:Ross,Sidney D.; Et Al
参考文献:Journal Of The American Chemical Society 日期:1955 卷标:77 页码:3020-3
1,2,3,4-Tetrahydro-9,10-Anthraquinone置于chromium(Vi) Oxide,Magnesium,溶剂黄146,锌体系中,化学反应生成 2-叔丁基蒽醌
参考文献:1,6-叔丁基氯化镁与蒽醌的加成反应
标题:1,6-叔丁基氯化镁与蒽醌的加成反应
摘要:叔丁基氯化镁和蒽醌之间的反应过程不同寻常.它给出了3,10-二叔丁基-10-羟基蒽酮作为主要的加成产物.进一步反应得到3,6,10-三叔丁基-10-羟基蒽酮.讨论了1,6-加成的这些及相关实例,以及格氏试剂作为碱所引起的竞争反应
DOI:10.1039/j39680001615
海关参考信息
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专利信息
专利号:US-4312811-A
优先权日:1979-09-13
标 题:Process for the production of substituted anthraquinones
发明人：SCHOEMANS JEAN; BOUILLET EDMOND
权利人:INTEROX SA
摘要:Substituted anthraquinones are obtained by thermal or catalytic dehydrochlorination of the corresponding substituted ortho-benzoylbenzoic acid chloride. n They may be used for the production of hydrogen peroxide and the synthesis of dyes.
专利号:US-2009227701-A1
优先权日:2004-08-19
标题:Water-soluble, radiation-curable products and use thereof
发明人：KRUEGER CHRISTIAN; BRUCHMANN BERND; HEES ULRIKE; KLUGE MICHAEL; DIELEMAN CEDRIC; WEISER JUERGEN
权利人:BASF AG
摘要:Water soluble radiation curable products (A) obtainable by mixingn mixing with or without reaction of at least one hyperbranched polyurethane (a) with at least one photoinitiator (b) or by synthesis of at least one hyperbranched polyurethane (a) in the presence of at least one photoinitiator (b),n nare used to produce aqueous inks for the ink jet process.
专利号:US-6103917-A
优先权日:1996-10-25
标 题:Method for regenerating anthraquinone derivatives during a synthesis process of hydrogen peroxide 30 %
发明人：LE LOARER JEAN-LUC; NEDEZ CHRISTOPHE; TAXIL BERNARD
权利人:PRO CATALYSE
摘要:PCT No. PCT/FR97/01909 Sec. 371 Date Jul. 27, 1999 Sec. 102(e) Date Jul. 27, 1999 PCT Filed Oct. 24, 1997 PCT Pub. No. WO98/18715 PCT Pub. Date May 7, 1998The invention concerns a method for regenerating a working solution for producing hydrogen peroxide 30%, in which the working solution is contacted with alumina at a temperature of approximately 40-160 DEG C.
专利号:US-7922940-B2
优先权日:2005-08-26
标题 :Preparation of silver particles using thermomorphic polymers
发明人：ITTEL STEVEN DALE
权利人:DU PONT
摘要:This invention relates to the synthesis and isolation of colloidal silver particles through the use of thermomorphic polymers and the resulting composition. It further relates to the use of the resulting composition in the preparation of inks for printing with silver-containing inks.
专利号:US-3998936-A
优先权日:1975-04-23
标题:Process for regenerating hydrogenation catalyst activity in hydrogen peroxide synthesis
发明人：ERNST RICHARD EDWARD; AMINI BIJAN; BAREFORD WILLIAM JOHN
权利人:DU PONT
摘要:Catalytic activity of a platinum group metal catalyst used in catalyzing the hydrogenation of a working solution of an alkylanthraquinone in a water-immiscible solvent in the manufacture of hydrogen peroxide, said catalyst having become at least partially inactivated, is regenerated by a process comprising contacting the catalyst in the presence of the working solution and in the absence of hydrogen with an oxidizing agent selected from the group consisting of an oxygen-containing gas and hydrogen peroxide. n When the process of the invention is made an integral part of the cyclic anthraquinone process for producing hydrogen peroxide, there results an improvement in the latter process whereby the activity of the catalyst can be maintained at a high level.
专利号:CA-2506422-A1
优先权日:2002-11-22
标题 :Enzymatic synthesis of polyol acrylates
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合成参考文献
摘要:Brasholz, M., Science of Synthesis: Photocatalysis in Organic Synthesis, (2018) 1, 383.
摘要:National Technical Information Service., OTS0556357
摘要:Chowdhury, D.; Koner, M.; Baidya, M., Science of Synthesis: Cross-Dehydrogenative Coupling, (2023) nan, 479.
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