CAS: 926-26-1; Di-Tert-Butyl Succinate
该化合物是丁基乙酸的一种异狄氏衍生物,其特点是其异丁基酯组的特性,该化合物由于受到阻塞的结构,具有高度的热和化学稳定性,因此适合对水解和氧化降解具有抗药性的应用,与各种聚合物的低挥发性和相容性增强了其作为塑料剂或特殊化学合成中间体的效用.
- 英文名称Di-Tert-Butyl Succinate
- 中文名称丁二酸二叔丁酯
- IUPAC名称di-tert-butyl succinate
- 其它别名Di-Tert-Butyl Succinate; Butanedioic Acid, Bis(1,1-Dimethylethyl) Ester; Ditert-Butyl Butanedioate; Butanedioic Acid, 1,4-Bis(1,1-Dimethylethyl) Ester
- CAS编号926-26-1
- MFCD编号:MFCD00127979
- FDA UNII编号:9U278DI8QD
- 分子式:C12H22O4
- 分子量:230.3
- 产品CID: 1964950
- 产品分类有机原料→分子砌块→脂肪链类化合物
相似化合物
3878-55-5 15026-17-2 110-15-6物理性质
上下游产品
丁二酸二甲酯 Dimethyl Succinate 106-65-0合成工艺路线路线简述
- 108-30-5 = 926-26-1
反应条件:1.1 Catalysts: Sulfuric Acid Solvents: Water
标题:Process And Aqueous Acid Catalysts For The Preparation Of Di-Tert-Butyl Succinate From Succinic Acid Or Anhydride And Isobutene
参考文献:European Patent Organization]
36805-97-7 + 110-15-6 = 926-26-1 [标题:Reaction Conditions
标题:A Convenient Preparation Of Tert-Butyl Esters
作者:Widmer,Ulrich
参考文献:Synthesis 日期:1983 卷标:(2) 页码:135-6]
106-65-0 = 926-26-1
反应条件:1.1 Catalysts: Cesium Carbonate,Lithium Hydroxide; Rt -> 83 °C; 24 H,82 - 83 °C; 76 - 78 °C
标题:Synthesis Of Di-Tert-Alkyl Succinate By Transesterification Under Catalysis Of Lithium Hydroxide And Cesium Carbonate
参考文献:China]
108-30-5 = 926-26-1
反应条件:1.1 Catalysts: Sulfuric Acid Solvents: Diisopropyl Ether,Toluene,Water; 2 H,30 °C1.2 Catalysts: Sulfuric Acid; 4 H,30 °C
标题:Process Of Manufacture Of Carboxylic Acid Tert-Butyl Esters
参考文献:Japan]
= 926-26-1
反应条件:1.1 Reagents: N,N-Dimethylaniline Solvents: Diethyl Ether; Reflux; 2 H,Reflux1.2 Reagents: Water
标题:Preparation Of Novel Peptide Nucleic Acid Monomers And Oligomers With Increased Thymidine Specificity
参考文献:World Intellectual Property Organization]
51656-70-3 = 926-26-1
反应条件:1.1 Catalysts: Tert-Butyl Bromoacetate
标题:A Reformatsky Reagent. Carbon-Carbon Bonds Formation By Substitution Reactions
作者:Orsini,F.; Pelizzoni,F.
参考文献:Synthetic Communications 日期:1983 卷标:13(6) 页码:523-30]
= 926-26-1 [标题:Reaction Conditions
标题:Reaction Of Ketone Enolates With Copper Dichloride. Synthesis Of 1,4-Diketones
作者:Ito,Yoshihiko; Konoike,Toshiro; Saegusa,Takeo
参考文献:Journal Of The American Chemical Society 日期:1975 卷标:97(10) 页码:2912-14]
= 926-26-1 [标题:Reaction Conditions
标题:General Preparative Method For The Esterification Of Carboxylic Acids With Isobutene In The Presence Of Tert-Butanol
作者:Pavlov,Slavka; Bogavac,Milica; Arsenijevic,Vladimir
参考文献:Bulletin De La Societe Chimique De France 日期:1974 卷标:(12) 页码:2985-6]
= 926-26-1 [标题:Reaction Conditions
标题:Self-Condensation Of α-Oxo Esters Under Stobbe Condensation Conditions
作者:Augustine,Robert L.; Calbo,Leonard P. Jr.
参考文献:Journal Of Organic Chemistry 日期:1968 卷标:33(2) 页码:838-40]
1621056-23-2 = 926-26-1
反应条件:1.1 Reagents: Chlorotrimethylsilane,Zinc; 1 H,Rt1.2 Catalysts: Tris(Dibenzylideneacetone)Dipalladium,X-Phos Solvents: Tetrahydrofuran; Overnight,Rt1.3 Reagents: Ammonium Chloride Solvents: Water; Rt
标题:3-Alkyl-1,2-Cyclopentanediones By Negishi Cross-Coupling Of A 3-Bromo-1,2-Cyclopentanedione Silyl Enol Ether With Alkylzinc Reagents: An Approach To 2-Substituted Carboxylic Acid γ-Lactones,Homocitric And Lycoperdic Acids
作者:Paju,Anne; Kostomarova,Diana; Matkevits,Katharina; Laos,Marit; Pehk,Tonis; Et Al
参考文献:Tetrahedron 日期:2015 卷标:71(49) 页码:9313-9320]
110-15-6 = 926-26-1
反应条件:1.1 Reagents: Poly(Acrylic Acid); 30 Min,120 °C
标题:Method For Obtaining Complex Di-Substituted Esters Of Some Dicarboxylic Acids C2-C10 With Monatomic Alcohols C4 Of Various Structures
参考文献:Russian Federation]
= 926-26-1
反应条件:1.1 Reagents: Lithium Diisopropylamide Solvents: Tetrahydrofuran,Hexane; -78 °C; 30 Min,-78 °C; 30 Min,Rt1.2 Catalysts: Zinc Chloride Solvents: Tetrahydrofuran; Rt; 30 Min,Rt1.3 Reagents: Oxygen Catalysts: Copper(Ii) Acetylacetonate; 10 Min,Rt
标题:Copper-Catalyzed Homodimerization Of Nitronates And Enolates Under An Oxygen Atmosphere
作者:Do,Hien-Quang; Tran-Vu,Hung; Daugulis,Olafs
参考文献:Organometallics 日期:2012 卷标:31(22) 页码:7816-7818]
= 926-26-1
反应条件:1.1 Solvents: Diethyl Ether; 2 H,Reflux1.2 Reagents: Water
标题:Synthesis Of Peptide Nucleic Acid Monomers And Triple-Helix Forming Oligomers With Non-Standard Bases For Thymidine Targeting In Nucleic Acid Hybridization
参考文献:United States]
= 926-26-1
反应条件:1.1 Reagents: N,N-Dimethylaniline Solvents: Diethyl Ether1.2 Solvents: Water
标题:1,8-Naphthyridin-2(1H)-Ones - Novel Bicyclic And Tricyclic Analogues Of Thymine In Peptide Nucleic Acids (Pnas)
作者:Eldrup,Anne B.; Nielsen,Bettina B.; Haaima,Gerald; Rasmussen,Hanne; Kastrup,Jette S.; Et Al
参考文献:European Journal Of Organic Chemistry 日期:2001 卷标:(9) 页码:1781-1790]
110-15-6 = 926-26-1
反应条件:1.1 Catalysts: Montmorillonite ((Al1.33-1.67Mg0.33-0.67)(Ca0-1Na0-1)0.33Si4(Oh)2O10.Xh2O) Solvents: Toluene; 8 H,Reflux
标题:Esterification Of Dicarboxylic Acids To Diesters Over Mn+-Montmorillonite Clay Catalysts
作者:Reddy,C. Ravindra; Iyengar,Pushpa; Nagendrappa,Gopalpur; Prakash,B. S. Jai
参考文献:Catalysis Letters 日期:2005 卷标:101(1-2) 页码:87-91]
= 926-26-1
反应条件:1.1 Catalysts: Lithium Diisopropylamide
标题:The Reaction Of Lithium α-Lithiocarboxylates (Dianions Of Carboxylic Acids) Or α-Lithiocarboxylic Esters (Ester Enolates) With α-Halocarboxylic Esters Or Lithium α-Halocarboxylates
作者:Petragnani,Nicola; Yonashiro,Massami
参考文献:Synthesis 日期:1980 卷标:(9) 页码:710-13]
= 926-26-1 [标题:Reaction Conditions
标题:Process For The Preparation Of Diesters Of Alkanedioic Acids
参考文献:European Patent Organization]
= 926-26-1 [标题:Reaction Conditions
标题:Dicarboxylate Ester From An Alkane And Carbon Monoxide
参考文献:European Patent Organization]
= 926-26-1 [标题:Reaction Conditions
标题:Ester Enolates. Ii. Preparation Of Di- And Tetrasubstituted Succinate Esters
作者:Brocksom,T. J.; Petragnani,N.; Rodrigues,R.; La Scale Teixeira,H.
参考文献:Synthesis 日期:1975 卷标:(6) 页码:396-7]
= 926-26-1 [标题:Reaction Conditions
标题:Reaction Of Ester Enolates With Copper(Ii) Salts. Synthesis Of Substituted Succinate Esters
作者:Rathke,Michael W.; Lindert,Andreas
参考文献:Journal Of The American Chemical Society 日期:1971 卷标:93(18) 页码:4605-6
醋酸叔丁酯置于zinc(II) Chloride,Lithium Diisopropyl Amide,Copper Acetylacetonate,氧气体系中,用 四氢呋喃 作为反应溶剂,化学反应 0.17H,以31%的收率获得产物丁二酸二叔丁酯
参考文献:Copper-Catalyzed Homodimerization Of Nitronates And Enolates Under An Oxygen Atmosphere
标题:Copper-Catalyzed Homodimerization Of Nitronates And Enolates Under An Oxygen Atmosphere
摘要:A Method For Copper-Catalyzed Oxidative Dimerization Of Nitronates And Enolates Using Oxygen As The Terminal Oxidant Has Been Developed. Cyclization Through Oxidative Intramolecular Coupling Is Also Feasible For Both Nitronates And Enolates. The Mild Reaction Conditions Lead To Good Functional Group Tolerance.
DOI:10.1021/om300393M
海关参考信息
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2905399002-1,4-丁二醇
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专利信息
专利号:EP-3491044-B1
优先权日:2016-07-27
标 题 :Method of regioselective synthesis of polyesters from asymmetric diols
专利号:US-2020181319-A1
优先权日:2016-07-27
标题:Method of regioselective synthesis of polyesters from asymmetric diols
专利号:US-11155675-B2
优先权日:2016-07-27
标 题:Method of regioselective synthesis of polyesters from asymmetric diols
发明人：NODARI MIRCO; LONGO ALDO; COLONNA MARTINO; GIOIA CLAUDIO
权利人:VERSALIS SPA
摘要:A method for synthesizing regioregular polyesters, starting from asymmetric diols, may provide the polymer ordered structure and advantageous physical-chemical properties. Such methods can make it is possible to obtain regioregular polyesters having high glass transition temperatures T g and crystalline properties. In the case in which the asymmetric diols are used in a pure enantiomeric form, with respect to the chiral carbon bound to the secondary hydroxyl, through the above-mentioned method it is possible to obtain regioregular and stereoregular polyesters, which may have thermal and crystalline properties further ameliorative with respect to non-chiral regioregular polymers.
专利号:CN-109689727-B
优先权日:2016-07-27
标题 :Process for the regioselective synthesis of polyesters from asymmetric diols
专利号:US-6723138-B2
优先权日:2000-06-07
标题 :Preparation of diketopyrrolopyrrole pigments
发明人：NICKEL UWE; UNVERDORBEN LEONHARD; WEBER JOACHIM; DIETZ ERWIN; PATZLAFF JUERGEN
权利人:CLARIANT INT LTD
摘要:A process for preparing diketopyrrolopyrrole pigments comprises conducting the elementary steps of pigment synthesis (reaction and hydrolysis) in a miniaturized continuous reactor.
专利号:KR-102397570-B1
优先权日:2016-07-27
标题 :Method of Regioselective Synthesis of Polyesters from Asymmetric Diols
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合成参考文献
参考文献:10.1007/s10562-004-3754-9
摘要:Reddy CR, Iyengar P, Nagendrappa G, Prakash BSJ. Esterification of dicarboxylic acids to diesters over Mn+-montmorillonite clay catalysts. Catalysis Letters. 2005 May;101(1-2):87–91. doi: 10.1007/s10562-004-3754-9.
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