CAS: 5323-87-5; 3-Ethoxy-2-Cyclohexen-1-One

相似化合物

16807-60-6 29941-82-0 7467-13-2

上下游产品

1,3-cylohexanedione ethyl iodide orthoformic acid triethyl ester ethanol 3-butylcyclohexenone 2'-methyl-5,6-dihydro-[1,1'-bi(phenyl)]-3(4H)-one 3-biphenyl-3-yl-cyclohex-2-enone 3-methylcyclohexen-2-one

3-丙氧基环己-2-烯-1-酮置于水体系中,用 乙腈 作为反应溶剂,20.0~80.0 °C,330.01 Kpa 条件下,反应 0.39H,反应生成 3-乙氧基-2-环己烯-1-酮
参考文献:连续流动条件下葡萄酒酯的快速和多克合成:葡萄酒酯的醚交换和逆反应
标题:连续流动条件下葡萄酒酯的快速和多克合成:葡萄酒酯的醚交换和逆反应
摘要:在廉价的amberlyst-15催化剂存在下,用醇类开发了一种从1,3-二酮合成乙烯基酯及其在连续流下逆反应的环境友好方法.这种方法学具有高度的选择性,对一系列环状的1,3-二羰基化合物具有通用性,在无溶剂和无金属的条件下,该文库可提供线性至烷基化和芳基化的乙烯基酯库,收率高至极佳.此外,在长达40小时的连续流中进行的长时间实验得到了8.0 G的乙烯基酯,其周转数(ton)= 28.6,周转频率(tof)= 0.715 H-1使用amberlyst-15作为催化剂.此外,已经以高收率实现了乙烯基酯与各种醇的连续流动顺序的醚交换.可逆地,使用环境友好的水作作为反应溶剂,使用amberlyst-15作为催化剂,在连续流过程中将该乙烯基酯脱保护或水解为酮.
DOI:10.1021/acs.Oprd.9B00067

专利信息

专利号:US-4585888-A
优先权日:1983-02-22
标 题 :Synthetic method for a chiral 3-(substituted-phenyl)-4-(3-hydroxypropyl)cyclohexanol
发明人：URBAN FRANK J
权利人:PFIZER
摘要:Racemic endo- and exo-1-methoxybicyclo[2.2.2]oct-5-ene-2-carboxylic acids are starting materials for a novel and efficient synthesis of chiral 3R-[2-hydroxy-4-(1,1-dimethylheptyl)phenyl]-4R-(3-hydroxypropyl)-1R-cyclohexanol, a compound having valuable central nervous system (CNS) activity, particularly as an analgesic and as an antiemetic.

专利号:US-7294748-B2
优先权日:2004-10-19
标 题:Sulfenic acid-reactive compounds and their methods of synthesis

专利号:US-2006084173-A1
优先权日:2004-10-19
标题:Sulfenic acid-reactive compounds and their methods of synthesis and use in detection or isolation of sulfenic acid-containing compounds

专利号:US-9868718-B2
优先权日:2006-01-06
标 题 :Cycloalkylamines as monoamine reuptake inhibitors
发明人：SHAO LIMING; WANG FENGJIANG; MALCOLM SCOTT CHRISTOPHER; HEWITT MICHAEL CHARLES; BUSH LARRY R; MA JIANGUO; VARNEY MARK A; CAMPBELL UNA; ENGEL SHARON RAE; HARDY LARRY WENDELL; KOCH PATRICK; CAMPBELL JOHN E
权利人:SUNOVION PHARMACEUTICALS INC
摘要:The invention relates to novel cyclohexylamine derivatives and their use in the treatment and/or prevention of central nervous system (CNS) disorders, such as depression, anxiety, schizophrenia and sleep disorder as well as methods for their synthesis. The invention also relates to pharmaceutical compositions containing the compounds of the invention, as well as methods of inhibiting reuptake of endogenous monoamines, such as dopamine, serotonin and norepinephrine from the synaptic cleft and methods of modulating one or more monoamine transporter.

专利号:US-2013288268-A1
优先权日:2004-10-19
标题:Sulfenic acid-reactive compounds and their methods of synthesis and use in detection or isolation of sulfenic acid-containing compounds

专利号:CN-117069555-A
优先权日:2023-07-31
标题 :A kind of synthesis method of substituted phenol