CAS: 1711-02-0; 4-Iodobenzoyl Chloride

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609-67-6 874-60-2 696-41-3

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CAS号619-58-9 对碘苯甲酸 | CAS号79-37-8 草酰氯 | CAS号106-37-6 对二溴苯 | CAS号6999-03-7 1-溴-4-三甲基硅基苯 | CAS号15290-29-6 4-(三甲基甲硅烷基)苯甲酸 | CAS号150-13-0 对氨基苯甲酸 | CAS号624-31-7 对碘甲苯 | CAS号106790-96-9 N-(2-(diethylam... | CAS号55794-28-0 4'-IODO-2-PHENY... | CAS号5748-41-4 4'-氯-[1,1'-联苯]-4-羧酸 | CAS号3815-20-1 4-联苯基甲酰胺 | CAS号141120-39-0 methyl (1S,3S,4... | CAS号187617-01-2 4-Iodo-N-methox... | CAS号205871-49-4 2'-甲酰基-[1,1'-联苯... | CAS号195436-88-5 2-(4-碘苯基)-噁唑 | CAS号92-92-2 4-苯基苯甲酸 | CAS号3469-20-3 2,3-二苯基吲哚

4-碘苯甲酸置于氯化亚砜体系中,用 二氯甲烷 用作溶剂,化学反应 8.0H,以99%的收率获得4-碘苯甲酰氯
参考文献:(L)-缬氨酸和(L)-缬氨醇在sba-15纳米多孔二氧化硅上的固定化及其作为手性异质配体在cu催化烯烃不对称烯丙基氧化中的应用
标题:(L)-缬氨酸和(L)-缬氨醇在sba-15纳米多孔二氧化硅上的固定化及其作为手性异质配体在cu催化烯烃不对称烯丙基氧化中的应用
摘要:以p123表面活性剂和原硅酸四乙氧基硅酸盐为原料,采用水热法合成sba-15纳米多孔二氧化硅,然后用3-氯丙基三甲氧基硅烷进行功能化.接下来,通过固定手性氨基酸(S)-2-氨基-3-甲基丁酸(l-缬氨酸)和手性氨基醇(S)-2-氨基-3-甲基丁烷-1-醇(l-缬氨醇)通过在 Thf 中通过 Nabh 4 /i 2还原l-缬氨酸制备,在功能化的 Sba-15 上,手性异质配体 Al*-I-Pr-Sba-15 和 Aa*-I-Pr-Sba-15 是通过 Ft-Ir,Xrd,Tga,Edx,Sem,Bet-Bjh 技术制备和表征.不对称烯丙基ic 烯烃的氧化是使用这些配体的铜配合物和合成的过酸酯完成的.通过改变各种参数如温度,溶剂,手性异质配体的量以及铜盐的类型和量来优化反应.在优化条件下,6 Mg Al*-I-Pr-Sba-15 和 3.2 Mol% Cu(Ch 3 Cn) 4 Pf 6在 50
Doi:10.1039/d1Nj02580E

专利信息

专利号:US-9035013-B2
优先权日:2010-08-04
标 题 :Sulphur-containing triazine monomer that can be used for the synthesis of a polymer membrane for a fuel cell
发明人：FEDURCO MILAN
权利人:FEDURCO MILAN; MICHELIN & CIE; MICHELIN RECH TECH
摘要:A sulphur-containing triazine monomer is provided that can be used in the synthesis of a polymer membrane for a PEM-type fuel cell. The sulphur-containing triazine monomer has a structure corresponding to a formula (I): n nin which:n Tz represents a 1,3,5-triazine nucleus; X 1 and X 2 , which are identical or different, represent S, SO, or SO 2 ; Ar 1 , Ar 2 , Ar 4 and Ar 5 , which are identical or different, represent a substituted or unsubstituted phenylene group; Ar 3 represents a substituted or unsubstituted phenyl group; and Z 1 and Z 2 , which are identical or different, are selected from a group that includes halogens, hydroxyl, alkoxyl, thiol, carboxyl, carboxylates, amine, sulphonamide, acyl chlorides, sulphonyl chlorides, sulphonyl fluorides, isocyanates, and combinations thereof.

专利号:US-6603070-B2
优先权日:2000-07-21
标题 :Convergent synthesis of multiporphyrin light-harvesting rods
发明人：LINDSEY JONATHAN S; LOEWE ROBERT S
权利人:UNIV NORTH CAROLINA STATE
摘要:The present invention provides a convergent method for the synthesis of light harvesting rods. The rods are oligomers of the formula A 1 (A b+1 ) b , wherein b is at least 1, A 1 through A b+1 are covalently coupled rod segments, and each rod segment A 1 through A 1+b comprises a compound of the formula X 1 (X m+1 ) m wherein m is at least 1 and X 1 through X m+1 are covalently coupled porphyrinic macrocycles. Light harvesting arrays and solar cells containing such light harvesting rods are also described, along with intermediates useful in such methods and rods produced by such methods.

专利号:US-7109377-B2
优先权日:1996-10-16
标 题:Synthesis of combinatorial libraries of compounds reminiscent of natural products
发明人：SCHREIBER STUART L; SHAIR MATTHEW D; TAN DEREK S; FOLEY MICHAEL A; STOCKWELL BRENT R
权利人:HARVARD COLLEGE
摘要:The present invention provides complex compounds reminiscent of natural products and libraries thereof, as well as methods for their production. The inventive compounds and libraries of compounds are reminiscent of natural products in that they contain one or more stereocenters, and a high density and diversity of functionality. In general, the inventive libraries are synthesized from diversifiable scaffold structures, which are synthesized from readily available or easily synthesizable template structures. In certain embodiments, the inventive compounds and libraries are generated from diversifiable scaffolds synthesized from a shikimic acid based epoxyol template. In other embodiments, the inventive compounds and libraries are generated from diversifiable scaffolds synthesized from the pyridine-based template isonicotinamide. The present invention also provides a novel ortho-nitrobenzyl photolinker and a method for its synthesis. Furthermore, the present invention provides methods and kits for determining one or more biological activities of members of the inventive libraries. Additionally, the present invention provides pharmaceutical compositions containing one or more library members.

专利号:EP-1641729-B1
优先权日:2003-07-09
标题:Use of functionalized onium salts as a soluble support for organic synthesis
发明人：VAULTIER MICHEL; GMOUH SAID; HASSINE FATIMA
权利人:CENTRE NAT RECH SCIENT; UNIV RENNES
摘要:The invention relates to the use of a onium salt functionalized by at least one organic function, as a soluble support, in the presence of at least one organic solvent, for organic synthesis of a molecule, in a homogenous phase, by at least one transformation of said organic function. The onium salt enables the synthesized molecule to be released. The onium salt is present in liquid or solid form at room temperature and corresponds to formula A₁⁺, X₁^-, wherein A₁⁺ represents a cation and X₁^- represents an anion.

专利号:US-6924375-B2
优先权日:2003-09-03
标题:Facile synthesis of 1,9-diacyldipyrromethanes
发明人：LINDSEY JONATHAN S; TAMARU SHUN-ICHI; YU LIANHE
权利人:UNIV NORTH CAROLINA STATE
摘要:The present invention provides a method of making a metal complex. The method comprises the steps of: (a) acylating a dipyrromethane or a 1-monoacyldipyrromethane to form a mixed reaction product comprising a 1,9-diacyidipyrromethane; (b) combining the reaction product with a compound of the formula R 2 MX 2 in the presence of a base, where R is alkyl or aryl, M is Sn, Si, Ge, or Pb (preferably Sn), and X is halo, OAc, acac, or OTf, to form a product comprising a metal complex of the formula DMR 2 in the mixed reaction product, wherein D is a 1,9-diacyldipyrromethane; and then (c) separating the metal complex from the mixed reaction product. The method may be utilized for the convenient synthesis and separation of 1,9-diacyldipyrromethanes. Metal complex intermediates useful in such methods are also described.

专利号:US-2003111108-A1
优先权日:2000-07-21
标题:Convergent synthesis of multiporphyrin light-harvesting rods