CAS: 393-01-1; 2,3,4-Trifluorobenzotrifluoride

上下游产品

CAS号872-50-4 N-甲基吡咯烷酮(NMP) | CAS号120770-03-8 2-氯-1,3-二氟-4-三氟甲苯 | CAS号126-33-0 环丁砜 | CAS号61841-45-0 1,2,3-trichloro... | CAS号115812-33-4 2,3,4-trifluoro... | CAS号124185-34-8 2,3-二氟-6-(三氟甲基)苯胺

2,3,4-三氟苯甲酸置于sulfur Tetrafluoride,氢氟酸体系中,化学反应 24.0H,以82%的收率获得2,3,4-三氟三氟甲苯
参考文献:(杂)芳族酸的脱氧氟化.
标题:(杂)芳族酸的脱氧氟化.
摘要:通过用四氟化硫对肉桂酸和(杂)芳族羧酸进行脱氧氟化反应,合成了不同的三氟甲基取代的化合物.所得产物用作制备新型氟化氨基酸,苯胺和脂肪胺的原料,这些氟化物是药物化学和农业化学的重要组成部分.
Doi:10.1021/acs.Joc.9B03011

专利信息

专利号:EP-0289036-A1
优先权日:1987-04-30
标题:Preparation of 3-chloro-4,5-difluorobenzotrifluoride
发明人：MUNDHENKE RUDOLPH F; TANG DAVID Y
权利人:OCCIDENTAL CHEM CO
摘要:In the synthesis of 3-chloro-4,5-difluorobenzotrifluoride by reaction of KF with 3,5-dichloro-4-fluorobenzotrifluoride, the production of undesirable by-products, especially over-fluorinated materials such as trifluorobenzotrifluoride is minimized when the reaction is run at a temperature of 196° to 206° Celsius in the presence of N-methyl-2-pyrrolidone.

专利号:CN-102311353-B
优先权日:2010-07-10
标 题 :Aldehyde group-containing polyaryletherketone monomer capable of post-functionalization and synthesis method thereof

专利号:CN-102311353-A
优先权日:2010-07-10
标 题:Aldehyde group-containing polyaryletherketone monomer capable of post-functionalization and synthesis method thereof