CAS: 6911-51-9; 1,2-Di(Thiophen-2-yl)Disulfane

上下游产品

CAS号3437-95-4 2-碘噻吩 | CAS号1003-09-4 2-溴噻吩 | CAS号16629-19-9 2-噻吩磺酰氯 | CAS号7774-74-5 2-噻吩硫醇 | CAS号2404-97-9 5-chlorothiophe... | CAS号188290-36-0 Thiophene(SIV) | CAS号7774-74-5 2-噻吩硫醇 | CAS号7774-73-4 3-巯基噻吩 | CAS号3807-37-2 2-(3-噻吩基硫代)噻吩 | CAS号3988-99-6 2-(2-噻吩基硫)噻吩 | CAS号16718-12-0 2-硫苯基噻吩

2-溴噻吩置于potassium Sulfide,Nickel(II) Chloride Hexahydrate,乙酰丙酮,Potassium Hydroxide体系中,用 水,N,N-二甲基甲酰胺 作为反应溶剂,化学反应 24.0H,以51%的收率获得产物双(2-噻吩基)二硫醚
参考文献:以硫化钾为硫源的镍催化对称合成二硫化物
标题:以硫化钾为硫源的镍催化对称合成二硫化物
摘要:摘要已经描述了一种从芳基和烷基卤化物和硫化钾合成有机二硫化物的有效的一锅法.k 2 S充当廉价且易于获得的硫源.使用nicl 2 .6H2O和乙酰丙酮作为催化体系,以非常好至极好的收率制备了各种对称的二芳基二芳基和二烷基二硫化物. 图形概要
DOI:10.1007/s00706-016-1673-2

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